Views: 1 Author: Site Editor Publish Time: 29-08-2022 Origin: Site
Properties
Melting point: 290℃
Boiling point: 479.59℃ (rough estimate)
Density: 0.998 g/cm3
Refractive index: 1.5300 (estimate)
Introduction
The crystal with green luster is reddish brown powder after grinding. Soluble in alcohol and dilute sodium hydroxide solution, slightly soluble in water.
Uses
Acid base reminder. Prepare 0.1% solution or 0.04% aqueous solution with 20% ethanol (take 0.04g of the product and dissolve it in 1.05ml of 0.1mnaoh solution), and then dilute it to 100ml. PH discoloration range: 7.2 (yellow) - 8.8 (purple); 2.0 (red) - 3.0 (Amber).
Production method
Mix benzenesulphonic anhydride, o-cresol and anhydrous zinc chloride, stir and heat, condense at 115-120 ℃ for about 7h, and purge the remaining o-cresol with steam. Filter, dissolve the filter cake with hot sodium carbonate aqueous solution, filter, neutralize with 1:1 hydrochloric acid in the clear filtrate, and stir vigorously. The crystals were filtered out, washed with a small amount of water and dried to obtain the finished product. If necessary, it can be purified by recrystallization of glacial acetic acid.